This is a specimen. It shows the layout, parameter structure, conformity
statements and declarations of a Praman certificate of analysis. The client, batch, results and accreditation
numbers are invented for illustration.
SPECIMEN
Unit 3, Sanjeevani Technology Park, Plot No. 14/B, MIDC Central Road
Andheri (East), Mumbai 400 093, Maharashtra, India
T +91 97110 84272
E labs@pramananalytical.in
W pramananalytical.in
Section A — Quality and composition All tests performed on the sample as received
#
Parameter
Unit
Test method
LOQ
Result
Specified limit
Conformity
1
Moisture †
% by mass
IS 1797 : 2017
0.10
7.24
10.0 max
Complies
2
Total ash †
% by mass
IS 1797 : 2017
0.10
6.12
9.0 max
Complies
3
Acid insoluble ash †
% by mass
IS 1797 : 2017
0.05
0.87
1.5 max
Complies
4
Crude fibre †
% by mass
IS 1797 : 2017
0.20
5.16
8.0 max
Complies
5
Volatile oil content †
mL/100 g
IS 1797 : 2017
0.10
2.64
1.5 min
Complies
6
Curcuminoids (as curcumin) †
% by mass
In-house PAL/CH/074, HPLC-PDA
0.05
3.82 ± 0.19
2.5 min
Complies
7
Starch, added (qualitative)
—
IS 1797 : 2017
—
Absent
Absent
Complies
8
Extraneous matter
% by mass
IS 1797 : 2017
0.05
0.11
1.0 max
Complies
PAL/COA/26/04417 · Specimen document
Continued overleaf — this report is valid only when all three pages are read together
Page 1 of 3
SPECIMEN
Report No. PAL/COA/26/04417
ULR TC884125000004417F
Page 2 of 3
Section C — Mycotoxins, residues and process contaminants
#
Parameter
Unit
Test method
LOQ
Result
Specified limit
Conformity
1
Aflatoxin B1 †
µg/kg
AOAC 2005.08, HPLC-FLD
0.50
< 0.50
5.0 max
Complies
2
Aflatoxins, total (B1+B2+G1+G2) †
µg/kg
AOAC 2005.08, HPLC-FLD
2.00
< 2.00
10.0 max
Complies
3
Ochratoxin A †
µg/kg
AOAC 2000.03, HPLC-FLD
1.00
< 1.00
20.0 max
Complies
4
Pesticide residues — 312 analyte screen †
mg/kg
QuEChERS, LC-MS/MS & GC-MS/MS Full analyte list at Annexure I
0.010
None detected above LOQ
As per FSSR, 2011
Complies
5
Ethylene oxide (sum as 2-chloroethanol) †
mg/kg
GC-MS/MS
0.010
< 0.010
0.1 max (EU)
Complies
Section D — Adulterants and non-permitted colours
#
Parameter
Unit
Test method
LOQ
Result
Specified limit
Conformity
1
Metanil yellow †
—
IS 1797 : 2017 / HPLC-PDA
1 mg/kg
Absent
Absent
Complies
2
Lead chromate †
—
IS 1797 : 2017
—
Absent
Absent
Complies
3
Sudan dyes I, II, III & IV †
mg/kg
LC-MS/MS
0.50
< 0.50
Absent
Complies
4
Synthetic colours, other †
—
IS 1797 : 2017 / HPLC-PDA
1 mg/kg
Absent
Absent
Complies
5
Chalk powder / foreign starch
—
Microscopic examination
—
Absent
Absent
Complies
6
Artificial colour on surface
—
Visual & solvent extraction
—
Absent
Absent
Complies
Section E — Microbiological examination Class 10,000 suite · analysis commenced within 24 h of receipt
#
Parameter
Unit
Test method
LOQ
Result
Specified limit
Conformity
1
Total plate count †
cfu/g
IS 5402 : 2012 / ISO 4833-1
10
1.2 × 10⁴
1.0 × 10⁵ max
Complies
2
Yeast & mould count †
cfu/g
IS 5403 : 1999 / ISO 21527
10
2.0 × 10²
1.0 × 10³ max
Complies
3
Coliforms †
cfu/g
IS 5401 (Part 1) : 2012
10
< 10
10 max
Complies
4
Escherichia coli †
per g
IS 5887 (Part 1) : 1976
—
Absent
Absent
Complies
5
Salmonella spp. †
per 25 g
ISO 6579-1 : 2017
—
Absent
Absent
Complies
6
Staphylococcus aureus †
cfu/g
IS 5887 (Part 2) : 1976
10
< 10
100 max
Complies
7
Bacillus cereus †
cfu/g
IS 5887 (Part 6) : 2012
10
< 10
10⁴ max
Complies
PAL/COA/26/04417 · Specimen document
Continued overleaf — opinion, declarations and authorisation
Page 2 of 3
SPECIMEN
Report No. PAL/COA/26/04417
ULR TC884125000004417F
Page 3 of 3
Opinion and interpretation
The sample described above, as received, complies with the requirements of the Food Safety
and Standards Regulations, 2011 (as amended) for turmeric powder, and with customer specification
SSE-QA-07 Rev. 4, for all parameters tested. No non-permitted colour, added starch or chromate-based
adulterant was detected. Pesticide residues were below the limit of quantification for all 312 analytes
screened; the sample additionally meets the European Union maximum residue level for ethylene oxide
expressed as 2-chloroethanol. This opinion is outside the scope of NABL accreditation and is offered at
the customer’s request.
Declarations, conditions and notes
The results relate only to the sample(s) as received and tested by the laboratory. Where sampling was
performed by the customer, the laboratory accepts no responsibility for the representativeness of the sample.
This report shall not be reproduced except in full, and shall not be used in any advertisement or for
product endorsement, without the prior written approval of the laboratory.
Parameters marked † are within the laboratory’s NABL accredited scope (Certificate TC-8841).
Parameters not so marked are performed under the laboratory’s quality system but are outside the
accredited scope.
Statements of conformity are made using a simple acceptance decision rule (guard band w = 0):
measurement uncertainty is not taken into account when the result is compared with the specified limit.
Expanded uncertainty, where reported, is stated at a coverage factor k = 2, corresponding to approximately
95 % confidence.
Results reported as “< value” indicate that the analyte was not detected at or above the
stated limit of quantification. “Absent” indicates a negative result by the qualitative method cited.
Remaining sample is retained for 30 days from the date of issue for non-perishable matrices and
7 days for perishable matrices, after which it is disposed of under documented procedure, unless
extended retention has been agreed in writing.
Any discrepancy in this report must be communicated to the Quality Manager in writing within
15 days of the date of issue. Appeals are handled by personnel not involved in the original work.
This report is issued subject to the laboratory’s standard terms of business and is not to be used
as evidence in a court of law except with the laboratory’s prior written consent.
The laboratory holds all information relating to this sample and this customer in confidence and does not
disclose it to any third party except where required by law.